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Do you need 1 dimensional or 2 dimensional NMR?
A combination of 1-dimensional and 2-dimensional NMR experiments are necessary for complete confidence in chemical structure. This post will walk you through the steps to fully characterize a molecule by 1- and 2-dimensional NMR, including on how to perform NMR interpretation.
How are carbon peaks determined in NMR spectroscopy?
Note that one of the carbons is hidden beneath the solvent signal but is clearly visible after zooming into that region. Distortionless Enhancement of Polarization Transfer (DEPT) experiments help assign carbon peaks by determining the number of protons attached to each carbon.
How does nuclear magnetic resonance ( NMR ) spectroscopy work?
Nuclear Magnetic Resonance (NMR) spectroscopy is an incredibly powerful tool for characterizing molecular structures. When submitting to the FDA or other regulatory agencies, full structural characterization by NMR provides crucial evidence of compound identity.
Which is the only aromatic proton in the NMR spectrum?
The integration and chemical shift support the assignment, as proton 4 is the only aromatic proton in the structure. There is only one singlet in the ¹H-NMR spectrum. The only proton that should show up as a singlet is proton 6, as it has no neighboring protons that would split the peak (the nearest proton is 5 bonds away!).
Last Update: Oct 2021
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